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Welcome BNE! Good to have you here!
You know, some folks would complain if you hung them with a new rope. If somebody is trying to dial in the exact exact EXACT alloy, it takes many samples to be sure you’re on solid ground. Nobody should take one test as gospel. If I wanted you to test one of my alloys, I would send you ten 1 pound ingots from the same batch, then average the results. That’s pretty much bullet proof if your machine is calibrated regularly.